Dimensional stability of two impression materials after a 6-month storage period

Francisco Martins; Patrícia Branco; José Reis; Ignacio Barbero Navarro; Paulo Maurício

doi:10.1080/23337931.2017.1401933

Authors

Francisco Martins Oral Rehabilitation Department, Instituto Superior de Ciências da Saúde Egas Moniz, Almada, Portugal
Patrícia Branco Oral Rehabilitation Department, Instituto Superior de Ciências da Saúde Egas Moniz, Almada, Portugal
José Reis Oral Rehabilitation Department, Instituto Superior de Ciências da Saúde Egas Moniz, Almada, Portugal
Ignacio Barbero Navarro Oral Medicine Department, Facultad de Odontología, Universidad de Sevilla, Sevilla, Spain
Paulo Maurício Oral Rehabilitation Department, Instituto Superior de Ciências da Saúde Egas Moniz, Almada, Portugal

DOI:

https://doi.org/10.1080/23337931.2017.1401933

Keywords:

Elastomers, sterilization, laser interferometry

Abstract

Objective: Oral rehabilitation success is enhanced by an accurate and reproducible final impression. The purpose of this study is to evaluate the dimensional changes of a polyether and addition silicone subjected to disinfection and/or sterilization after a long storage period.

Material and methods: Ninety samples were obtained from polyether Impregum^TM Penta^TM (3M ESPE^TM, Seefeld, Germany) and 90 of addition silicone Imprint^TM 4 Penta^TM Putty (3M ESPE^TM, Seefeld, Germany) according to ISO 4823:2000. The samples of each material were split to form three groups with 30 samples each: a control group, a hypochlorite group (disinfection) and an autoclave group (sterilization). Samples were stored in the Portuguese Institute for Quality for six months at 23 °C. Samples were measured by laser interferometry, according to the Michelson technique before calculating dimensional stability according ISO 4823:2000. A statistical analysis via a three-way mixed ANOVA was performed.

Results: Significant shrinkage of Impregum^TM Penta^TM was 0.77 ± 0.17% in the control group, 0.42 ± 0.19% in the hypochlorite group and 0.52 ± 0.28% in the autoclave group. For Imprint^TM 4 Penta^TM Putty, the control group had a shrinkage of 0.42 ± 0.12%, the hypochlorite group 0.36 ± 0.09% and the autoclave group 0.59 ± 0.13%.

Conclusions: The long-term storage of samples subjected to disinfection with 5.25% hypochlorite or autoclave sterilization can be used in a clinical setting as the dimensional changes are below the maximum permitted by the ISO 4823:2000, since there are no clinically significant changes in the dimension of the samples during the storage period.