Effect of food-simulating liquids on flexural strength, Vickers microhardness, and surface roughness of IPS e.max Press and CEREC Tessera

Authors

  • Asmaa Abdeewi Libyan Polymer Research Center, Tripoli, Libya; Research and Consultancy Center, Sirte University, Tripoli, Libya
  • Seham A. Elsawaay Fixed Prosthodontics Department, Faculty of Dentistry, University of Tripoli, Tripoli, Libya
  • Ahmed A. Mhanni Fixed Prosthodontics Department, Faculty of Dentistry, University of Tripoli, Tripoli, Libya
  • Abubaker Qutieshat Restorative Dentistry, College of Dental Medicine, University of Sharjah, Sharjah, UAE

DOI:

https://doi.org/10.2340/biid.v13.46275

Keywords:

Ceramics, citric acid, ethanol, saliva, artificial, flexural strength, mechanical tests, surface properties

Abstract

Background: Lithium disilicate ceramics are widely used for indirect restorations, yet their mechanical performance may be influenced by fabrication route and chemical challenge from foods and beverages.

Objective: To compare the effects of food-simulating liquids (FSLs) on flexural strength, Vickers microhardness, and surface roughness of pressed lithium disilicate (IPS e.max Press) and Computer-Aided Design and Computer-Aided Manufacturing (CAD/CAM) advanced lithium disilicate (CEREC Tessera).

Materials and methods: One hundred fifty rectangular specimens were prepared using IPS e.max Press and CEREC Tessera (n = 75 each) and allocated into five groups per material (n = 15): one unconditioned control group, artificial saliva (7 days at 37°C), 0.02% citric acid, 20% ethanol, or 50% ethanol. Citric acid and ethanol groups underwent three 5-minute challenge cycles followed by re-storage in artificial saliva. Flexural strength was assessed by three-point bending. Microhardness (Vickers HV1/10) and surface roughness (Ra) were measured on independent specimens. Data were analysed using two-way analysis of variance with Tukey’s post hoc test for flexural strength and surface roughness. For microhardness, factorial analysis was limited to the comparable shared conditions because ethanol-exposed IPS e.max Press specimens did not yield reliable Vickers measurements.

Results: CEREC Tessera showed higher flexural strength than IPS e.max Press across conditions (control: 362.6 ± 15.4 vs 331.0 ± 8.5 MPa). Ethanol reduced strength in both materials, with the greatest reduction in 50% ethanol (238.0 ± 9.6 vs 147.4 ± 7.5 MPa). Across comparable conditions, CEREC Tessera also showed higher microhardness, while reliable Vickers measurements could not be obtained for ethanol-exposed IPS e.max Press specimens. Surface roughness increased after acidic and alcoholic exposure in both materials, although CEREC Tessera remained smoother overall (control: 0.06 ± 0.02 vs 0.67 ± 0.36 µm).

Conclusion: CEREC Tessera demonstrated superior flexural strength, microhardness, and surface integrity compared with IPS e.max Press after exposure to FSLs, suggesting that fabrication route influences laboratory performance under chemical challenge.

Downloads

Download data is not yet available.

References

Al-Johani H, Bukhari A, Abduo J, Sulaiman T. Effect of food-simulating solvents on the stainability and mechanical properties of partially and fully crystallized lithium disilicate glass-ceramics. J Prosthet Dent. 2025;134(6):2560.e1–e9 DOI: https://doi.org/10.1016/j.prosdent.2025.08.015

Alhindi S, Oliveira D, Pereira P, Elkaffas AA, Rocha M. Biaxial flexural strength of lithium‐based CAD/CAM dental glass‐ceramics. J Esthet Restor Dent. 2026;38(4):837–45 DOI: https://doi.org/10.1111/jerd.70081

Tang X, Tang C, Su H, Luo H, Nakamura T, Yatani H. The effects of repeated heat-pressing on the mechanical properties and microstructure of IPS e. max Press. J Mech Behav Biomed Mater. 2014;40:390–6 DOI: https://doi.org/10.1016/j.jmbbm.2014.09.016

Stawarczyk B, Meinen J, Wuersching SN. Two-body wear of novel monolithic lithium-silicate ceramic materials and their corresponding different antagonists. J Dent. 2024;144:104952 DOI: https://doi.org/10.1016/j.jdent.2024.104952

Abd El Hhaaliem NN, Elguindy J, Zaki AA. A one-year clinical evaluation of IPS E. max press versus CERASMART endocrowns in anterior endodontically treated teeth: a randomised clinical. Braz Dent Sci. 2021;24:1–13 DOI: https://doi.org/10.14295/bds.2021.v24i3.2414

Kandil MT, Zohdy MM, Zaky MS. Flexural strength and hardness of different lithium disilicate ceramics after variable crystallization speed: an in-vitro study. Ain Shams Dent J. 2025;39:12–20 DOI: https://doi.org/10.21608/asdj.2025.360209.1858

Alkadi L, Ruse ND. Fracture toughness of two lithium disilicate dental glass ceramics. J Prosthetic Dent. 2016;116:591–6 DOI: https://doi.org/10.1016/j.prosdent.2016.02.009

Wang RR, Lu CL, Wang G, Zhang DS. Influence of cyclic loading on the fracture toughness and load bearing capacities of all-ceramic crowns. Int J Oral Sci. 2014;6:99–104 DOI: https://doi.org/10.1038/ijos.2013.94

Awad OM, Hameed MR. Effect of hydrofluoric acid etching time on flexural strength and surface roughness of CAD/CAM ceramic materials. Jordan Med J. 2025;59:136 DOI: https://doi.org/10.35516/jmj.v59i1.2602

Zogheib LV, Bona AD, Kimpara ET, Mccabe JF. Effect of hydrofluoric acid etching duration on the roughness and flexural strength of a lithium disilicate-based glass ceramic. Braz Dent J. 2011;22:45–50 DOI: https://doi.org/10.1590/S0103-64402011000100008

Jurado CA, Arndt K, Azpiazu-Flores FX, Faddoul F, França R, Fischer NG, et al. Evaluation of glazing and polishing systems for novel chairside CAD/CAM lithium disilicate and virgilite crowns. Oper Dent. 2023;48:689–99 DOI: https://doi.org/10.2341/23-017-L

Lu Y, Dal Piva AO, Nedeljkovic I, Tribst JM, Feilzer AJ, Kleverlaan CJ. Effect of glazing technique and firing on surface roughness and flexural strength of an advanced lithium disilicate. Clin Oral Investig. 2023;27:3917–26 DOI: https://doi.org/10.1007/s00784-023-05014-1

Al-Johani H, Al-Amoudi A, Di Fiore A, Zhang Y. The effect of food-simulating liquids on the mechanical properties of lithium aluminosilicate glass-ceramics. Dent Mater. 2025;42:138–44 DOI: https://doi.org/10.1016/j.dental.2025.09.015

Al-Thobity AM, AlOtaibi AM, Alhumaidan AE, Aldossary AA, Siddiqui IA, Helal MA, et al. Impact of thermocycling on surface roughness, microhardness and optical properties of three different lithium disilicate ceramics. Saudi Dent J. 2022;34:589–95 DOI: https://doi.org/10.1016/j.sdentj.2022.08.004

Vechiato-Filho AJ, Dos Santos DM, Goiato MC, Moreno A, De Medeiros RA, Kina S, et al. Surface degradation of lithium disilicate ceramic after immersion in acid and fluoride solutions. Am J Dent. 2015;28:174–80.

Bresser RA, Hofsteenge JW, Buijs GJ, van den Breemer CR, Özcan M, Cune MS, et al. Partial glass-ceramic posterior restorations with margins beyond or above the cemento-enamel junction: an observational retrospective clinical study. J Prosthodont Res. 2024;69:49–57 DOI: https://doi.org/10.2186/jpr.JPR_D_23_00219

Silva LS, Bento VA, Cruz KH, Nascimento VA, Pesqueira AA, Pellizzer EP. Effect of gastric juice on the surface, optical, and mechanical properties of different computer-aided design/computer-aided manufacturing dental ceramics: a systematic review and meta-analysis. J Indian Prosthodont Soc. 2025;25:109–19 DOI: https://doi.org/10.4103/jips.jips_81_24

Al-Johani H, Haider J, Satterthwaite J, Silikas N. Lithium silicate-based glass ceramics in dentistry: a narrative review. Prosthesis. 2024;6:478–505 DOI: https://doi.org/10.3390/prosthesis6030034

Yanıkoğlu ND, Sakarya RE. Test methods used in the evaluation of the structure features of the restorative materials: a literature review. J Mater Res Technol. 2020;9(5):9720–34 DOI: https://doi.org/10.1016/j.jmrt.2020.06.049

Fusayama T, Katayori T, Nomoto S. Corrosion of gold and amalgam placed in contact with each other. J Dent Res. 1963;42:1183–97 DOI: https://doi.org/10.1177/00220345630420051301

Qutieshat AS, Mason AG, Chadwick RG. Informing a realistic laboratory erosion-testing regime-observations. J Dent. 2015;43:1352–7 DOI: https://doi.org/10.1016/j.jdent.2015.08.008

Pytko-Polonczyk J, Jakubik A, Przeklasa-Bierowiec A, Muszynska B. Artificial saliva and its use in biological experiments. J Physiol Pharmacol. 2017;68:807–13.

International Organization for Standardization (ISO). ISO 6872:2024 dentistry – ceramic materials. Geneva: ISO; 2024.

International Organization for Standardization. ISO 6507-1: metallic materials – Vickers hardness test – part 1: test method 2018. Geneva: ISO; 2018.

ASTM International. ASTM C1327-15: standard test method for Vickers indentation hardness of advanced ceramics 2015. West Conshohocken, PA: ASTM International; 2015.

Jurado CA, Yeh JS, Vidal CM, Cho SH, Abuhammoud S. Fracture load of chairside CAD‐CAM veneers fabricated with pre‐and fully crystalized lithium disilicate ceramics. J Prosthodont. 2025;34:429–35 DOI: https://doi.org/10.1111/jopr.13867

Elraggal A, Afifi RR, Alamoush RA, Raheem IA, Watts DC. Effect of acidic media on flexural strength and fatigue of CAD-CAM dental materials. Dent Mater. 2023;39:57–69 DOI: https://doi.org/10.1016/j.dental.2022.11.019

Eser M, Çelik Öge S, Ekren O. Effect of food-simulating liquids on the mechanical properties of 3D-printed provisional restoration materials. Int J Prosthodont. 2024;37:71 DOI: https://doi.org/10.11607/ijp.8869

Sagsoz O, Sagsoz NP. Chemical degradation of dental CAD/CAM materials. Biomed Mater Eng. 2019;30:419–26 DOI: https://doi.org/10.3233/BME-191063

Alnasser M, Finkelman M, Papathanasiou A, Suzuki M, Ghaffari R, Ali A. Effect of acidic pH on surface roughness of esthetic dental materials. J Prosthet Dent. 2019;567:e1–8 DOI: https://doi.org/10.1016/j.prosdent.2019.08.022

Kukiattrakoon B, Hengtrakool C, Kedjarune-Leggat U. Effect of acidic agents on surface roughness of dental ceramics. Dent Res J. 2011;8:6–15.

Gökay D, Oyar P, Durkan D. Impact of various aging treatments on the microhardness and surface roughness of CAD-CAM monolithic restorative materials. J Prosthodont. 2025;34(9):977–87 DOI: https://doi.org/10.1111/jopr.13846

Ozdogan A, Ozdemir H. Effects of multiple firing processes on the mechanical properties of lithium disilicate glass-ceramics produced by two different production techniques. J Prosthet Dent. 2021;125:527–e1 DOI: https://doi.org/10.1016/j.prosdent.2020.10.016

Downloads

Published

2026-06-23

How to Cite

Abdeewi, A., Elsawaay, S. A., Mhanni, A. A., & Qutieshat, A. (2026). Effect of food-simulating liquids on flexural strength, Vickers microhardness, and surface roughness of IPS e.max Press and CEREC Tessera. Biomaterial Investigations in Dentistry, 13(1), 499–507. https://doi.org/10.2340/biid.v13.46275